Oil solution

silicone resin

16.0 g

ethyl acetate

4.0 g

hardening agent

1.6 g

surfactant (Span 80)

1.0 g

Inner aqueous solution

distilled water

3 ml

ethyl alcohol

2 ml

Continuous water phase

distilled water

300 ml

surfactant

12.0 g

revolution speed

6.7 s−1

Reaction condition

temperature

70˚C

reaction time

3 h

revolution speed

5 s−1

Drying-in-liquid condition

temperature

room temperature

revolution speed

11.7 s−1